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Absolute asymmetric synthesis of five-coordinate complexes

Journal article
Authors Anders Lennartson
Mikael Håkansson
Published in New Journal of Chemistry
Volume 39
Issue 8
Pages 5936-5943
ISSN 1144-0546
Publication year 2015
Published at Department of Chemistry and Molecular Biology
Pages 5936-5943
Language en
Links dx.doi.org/10.1039/c5nj00254k
Subject categories Chemical Sciences

Abstract

In 2009, we reported the first example of the optical resolution of a five-coordinate complex. In this study, we discuss the chirality of five-coordinate enantiomers displaying mono- and bi-dentate ligands by optical resolution of three complexes. Through total spontaneous resolution, it was possible to obtain optically active bulk products starting from achiral precursors only. It was discovered that crystallisation of two of the complexes was influenced by undetectable amounts of an unidentified source of optical activity.

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